143650
5H-二苯并[b,f]氮杂
97%
别名:
亚氨基芪
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关于此项目
经验公式（希尔记法）:
C14H11N
化学文摘社编号:
分子量:
193.24
UNSPSC Code:
12352100
NACRES:
NA.22
PubChem Substance ID:
EC Number:
205-970-0
Beilstein/REAXYS Number:
1343358
MDL number:
Assay:
97%
mp
196-199 °C (lit.)
solubility
ethyl acetate: soluble 25 mg/mL, clear, yellow to orange
InChI key
LCGTWRLJTMHIQZ-UHFFFAOYSA-N
InChI
1S/C14H11N/c1-3-7-13-11(5-1)9-10-12-6-2-4-8-14(12)15-13/h1-10,15H
SMILES string
N1c2ccccc2C=Cc3ccccc13
assay
97%
Quality Level
General description
5H-二苯并[b,f]吖庚因是一种具有七元环的三环类胺，常称为亚氨基芪。它可用作合成多种抗痉挛药物的中间体或起始材料。
Application
5H-二苯并[b,f]氮杂卓可用于：
- 作为原料制备重要的二苯并氮杂卓-哒嗪衍生物。
- 合成氨基苯酚衍生物制备中的关键中间体 3-氯-1-(5H-二苯并[b,f]氮杂卓-5基)丙烷-1-酮。
- 合成二苯并氮杂卓衍生物。
- 作为原料合成用于制备铑（I）配合物的烯类多齿配体。
Biochem/physiol Actions
2-（溴甲基）萘是一种荧光烷基溴。它通过酶水解使聚对苯二甲酸乙二醇酯表面形成的游离羧基酯化。它在P4S10/酰基胞苷反应中充当有机亲电子试剂。
signalword
Warning
hcodes
Hazard Classifications
Acute Tox. 4 Oral - Aquatic Chronic 2
存储类别
11 - Combustible Solids
wgk
WGK 2
flash_point_f
Not applicable
flash_point_c
Not applicable
ppe
dust mask type N95 (US), Eyeshields, Gloves
Synthesis and Calorimetry of Some Derivatives of Dibenzazepine
Analytical Calorimetry (1970)
Rh (I) Complex with a Tridentate Pyridine-Amino--Olefin Actor Ligand-Metal-Ligand Cooperative Activation of CO2 and Phenylisocyanate under C-C and Rh-E (E=O, N) Bond Formation
Heuermann I, et al.
Organometallics, 38(8), 1787-1799 (2019)
Kuppuswamy Arumugam et al.
Inorganic chemistry, 46(8), 3283-3288 (2007-03-16)
The reaction of P4S10 with acyloins, RC(O)CH(OH)R, in refluxing dioxane, followed by the addition of alkylating agents, forms dithiolene thiophosphoryl thiolate compounds, (R2C2S2)P(S)(SR'), which are readily isolated and purified. The compounds that have been prepared and identified spectroscopically are those
Synthesis of N-substituted dibenzoazepine--pyridazine derivatives as potential neurologically active drugs
Erdougan M and Dacstan A
Synthetic Communications, 50(24), 1-9 (2020)
Synthesis and antioxidant properties of some novel 5H-dibenz [b, f] azepine derivatives in different in vitro model systems
Kumar HV and Naik N
European Journal of Medicinal Chemistry, 45(1), 2-10 (2010)
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