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应用
用于制备以下化合物的反应物：
用于以下反应的试剂：
- 免疫刺激剂 α-半乳糖神经酰胺
- 纤维三糖和纤维四糖类似物，作为过渡态模拟物，用于纤维素酶的机理研究
- 双底物抑制剂，在儿茶酚-O-甲基转移酶的活性位点具有分子识别功能
- 具有大麻素 CB1 受体结合活性的 F200 和 S383 的衍生物
- 氮杂-β-内酰胺，通过 NHC 催化乙烯酮 [2 + 2] 环加成反应
用于以下反应的试剂：
- N-保护亚胺的环化
- α-可硫醇化的酮与硫氰酸铵的硫氰酸化
- Diels-Alder 反应
Diethyl azodicarboxylate (DEAD) is a reagent used in the Mitsunobu reaction.
DEAD can also be used as a reagent in the:
DEAD can also be used as a reagent in the:
- Synthesis of esters, ethers, amines, and thioethers of alcohols.
- Oxidation of alcohols to carbonyl derivatives using ZnBr2 as a catalyst via dehydrogenation reaction.
- Conversion of alcohol to an azide key intermediate in the total synthesis of immunostimulant α-galactosylceramides.
- Synthesis of aza-β-lactams from aryl(alkyl)ketenes.
- Synthesis of 1H-1,2,4-triazole-1,4(5H)-dicarboxylate derivatives.
- Diels-Alder type reactions.
其他说明
用于 Mitsunobu 反应的试剂，综述
警示用语：
Danger
危险分类
Aquatic Chronic 3 - Asp. Tox. 1 - Eye Irrit. 2 - Flam. Liq. 3 - Repr. 2 - Skin Irrit. 2 - STOT RE 2 - STOT SE 3
靶器官
Central nervous system, Respiratory system
储存分类代码
3 - Flammable liquids
WGK
WGK 3
闪点(°F)
105.8 °F - closed cup
闪点(°C)
41 °C - closed cup
个人防护装备
Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter
法规信息
新产品
Synthesis and thermolysis of Diels-Alder adducts of 2, 9-dialkylpentacenes with diethyl azodicarboxylate
Okamoto K, et al.
Journal of Physical Organic Chemistry, 21(3), 257-262 (2008)
The Mitsunobu reaction: origin, mechanism, improvements, and applications
But TYS and TPH
Chemistry - An Asian Journal, 2(11), 1340-1355 (2007)
Enantioselective synthesis of aza-β-lactams via NHC-catalyzed [2+ 2] cycloaddition of ketenes with diazenedicarboxylates
Huang X-L, et al.
The Journal of Organic Chemistry, 74(19), 7585-7587 (2009)
The Total Synthesis of Immunostimulant α-Galactosylceramides from Naturally Configured α-Galactoside Raffinose
Zhang Z, et al.
Organic Letters, 13(17), 4530-4533 (2011)
Oxime-based linker libraries as a general approach for the rapid generation and screening of multidentate inhibitors
Bahta M, et al.
Nature Protocols, 7(4), 686-686 (2012)
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