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394904

Supelco

Pentafluoropropionic anhydride

LiChropur™, 99%

Synonym(s):

PFPA, Perfluoropropionic anhydride

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1 KIT
¥8,017.76

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1 KIT
¥8,017.76

About This Item

Linear Formula:
(CF3CF2CO)2O
CAS Number:
356-42-3
Molecular Weight:
310.05
Beilstein:
1806446
EC Number:
206-604-2
MDL number:
MFCD00000429
UNSPSC Code:
23151817
PubChem Substance ID:
329755875
NACRES:
NA.22

¥8,017.76

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grade

derivatization grade ((GC derivatization))

Quality Level

100

Assay

99%

form

liquid

quality

LiChropur™

reaction suitability

reagent type: derivatization reagent
reaction type: Acylations

technique(s)

gas chromatography (GC): suitable

bp

69-70 °C/735 mmHg (lit.)

density

1.571 g/mL at 25 °C (lit.)

SMILES string

FC(F)(F)C(F)(F)C(=O)OC(=O)C(F)(F)C(F)(F)F

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Headspace vial, screw top, rounded bottom (vial only) volume 20 mL, clear glass vial, thread for 18, O.D. × H 22.5 mm × 75.5 mm, pkg of 100 ea

SU860097

Headspace vial, screw top, rounded bottom (vial only)

Headspace vial, screw top, rounded bottom (vial only) volume 20 mL, amber glass vial, thread for 18, O.D. × H 22.5 mm × 75.5 mm, pkg of 100 ea

SU860098

Headspace vial, screw top, rounded bottom (vial only)

Headspace vial, screw top, rounded bottom (vial only) volume 10 mL, clear glass vial, thread for 18, O.D. × H 22.5 mm × 46 mm, pkg of 100 ea

SU860099

Headspace vial, screw top, rounded bottom (vial only)

Headspace vial, beveled top, rounded bottom volume 20 mL, clear glass vial, O.D. × H × I.D. 23 mm × 75.5 mm × 12.5 mm, for use with PerkinElmer, pkg of 100 ea

SU860049

Headspace vial, beveled top, rounded bottom

material

clear glass vial, round bottom

material

amber glass vial, round bottom

material

clear glass vial, round bottom

material

clear glass vial, round bottom

fitting

thread for 18

fitting

thread for 18

fitting

thread for 18

fitting

thread for 20 mm

volume

20 mL

volume

20 mL

volume

10 mL

volume

20 mL

compatibility

for use with CTC PAL (Varian, Gerstel, Atas, Shimadzu)

compatibility

for use with CTC PAL (Varian, Gerstel, Atas, Shimadzu)

compatibility

for use with CTC HTC PAL, for use with CTC PAL (Varian, Gerstel, Atas, Shimadzu)

compatibility

for use with PerkinElmer

packaging

pkg of 100 ea

packaging

pkg of 100 ea

packaging

pkg of 100 ea

packaging

pkg of 100 ea

Application

Learn more in the Product Information
Derivatization reagent used in a GC-MS analysis of stereoisomer content of synthetic peptides.[1] Also used in a GC-MS detection method for synephrine in dietary supplements.[2]
For the preparation of volatile pentafluoropropionyl derivatives of a wide range of compounds, for example, amines and alcohols, for EC/GC.
Pentafluoropropionic anhydride (PFPA) was used as derivatization reagent for urine samples to determine the presence of codeine, morphine, 6-monoacetylmorphine, ethylmorphine, and dihydrocodeine using GC-MS in selected ion monitoring (SIM) mode.[3] It was also used to derivatize the dry pericardial fluid sample extracts for quantification of cocaine, benzoylecgonine, and cocaethylene in pericardial fluid using GC-MS.[4]

Packaging

Clear borosilicate glass, high hydrolytic resistance (Type I)

Legal Information

LiChropur is a trademark of Merck KGaA, Darmstadt, Germany

Pictograms

Corrosion
GHS05

Signal Word

Danger

Hazard Statements

H314

Precautionary Statements

P280 - P305 + P351 + P338 - P310

Hazard Classifications

Skin Corr. 1B

Supplementary Hazards

EUH014

Storage Class Code

8A - Combustible corrosive hazardous materials

WGK

WGK 3

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable

Personal Protective Equipment

dust mask type N95 (US), Eyeshields, Gloves

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    Certificates of Analysis (COA)

    Lot/Batch Number
    BCCM5270
    BCCL9144
    BCCK6300
    BCCH6332
    BCCG2902

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    Emilia Marchei et al.
    Journal of pharmaceutical and biomedical analysis, 41(4), 1468-1472 (2006-05-16)
    A simple and rapid procedure based on gas chromatography-mass spectrometry (GC-MS) is described for determination of synephrine, active principle of Citrus aurantium plant, in solid and liquid dietary supplements. After the addition of 3,4-methylenedioxypropylamphetamine as internal standard (I.S.), a liquid-liquid
    Ralf Pätzold et al.
    Chirality, 18(7), 551-557 (2006-05-10)
    Synthetic dipeptides comprising mixtures of enantiomers, diastereomers, or sequential isomers were converted into their N-perfluoroacetyl dipeptide esters (perfluoroacetyl: trifluoroacetyl, pentafluoroacetyl, heptafluorobutyryl; ester: methyl, 1-propyl, 2-propyl, 2,2,2-trifluoroethyl) and analyzed by GC-MS on the chiral stationary phases Chirasil-L-Val and Lipodex-E using helium
    María Teresa Contreras et al.
    Journal of analytical toxicology, 31(2), 75-80 (2007-06-01)
    A method is described for the simultaneous quantification of cocaine, benzoylecgonine, and cocaethylene in pericardial fluid. Pericardial fluid samples from autopsy casework involving cocaine-related deaths and deaths unrelated to drug abuse were collected. The extraction of cocaine and its metabolites
    Comparison of RapiTest? with Emit? d, au? and GC-MS for the Analysis of Drugs in Urine.
    Korte, T., et al.
    Journal of Analytical Toxicology, 21, 49-53 (1997)
    K Takamoto et al.
    European journal of biochemistry, 228(2), 362-372 (1995-03-01)
    An accurate carboxy-terminal sequencing method has long been sought to complement the Edman degradation procedure for amino-terminal amino acid sequence analysis. The method presented here is a unique and simple method to partly fulfill the needs. Exposure of a polypeptide
    View All Related Papers

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