KITALYSIS-CN
KitAlysis™ High-Throughput Buchwald-Hartwig Amination Reaction Screening Kit-Pack of 4
Synonym(s):
Amination Screening Kit, Buchwald-Hartwig Amination
About This Item
reaction suitability
reaction type: Buchwald-Hartwig Amination
reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Cross Couplings
reagent type: catalyst
core: palladium
storage temp.
room temp
General description
Application
Two Solvents, Weak Base (Cs2CO3)
Download the experimental excel file here
Two Solvents, Strong Base (NaOt-Bu)
Download the experimental excel file here
One Solvent (Dioxane), Two Bases
Download the experimental excel file here
One Solvent (DMAc), Two Bases
Download the experimental excel file here
Each kit contains 4 screening sets that contain the following:
Each customizable screening kit contains
- 12 X 2 pre-weighed catalysts (1 μmol) in individual microvials with magnetic stir bars
- 2 bases (NaOt-Bu and Cs2CO3)
- 2 degassed anhydrous solvents (dioxane and DMAc) in ampules
- 2 substrate reaction vials with stir bars
- 1 internal standard
- 4 reaction block replacement films
Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).
Features and Benefits
- Designed and tested by synthetic chemists
- Easily run 24-microscale reaction in parallel
- 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration
- Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks
Legal Information
Kit Components Only
- SnapIT Ampule Opener, Regular, for 1-2ml, 5-10ml, 10-15ml ampoules 1 EA
Kit Components Also Available Separately
- 900634N,N-Dimethylacetamide, anhydrous, ZerO2®, 99.8% 8 mLSDS
- 9006401,4-Dioxane, anhydrous, ZerO2®, 99.8% 8 mLSDS
- 702706Sodium tert-butoxide solution, 2 M in THF, ZerO2® 4 mLSDS
- 747130Josiphos SL-J009-1 Pd G3 5 µmolSDS
- 753009SPhos Pd G2 5 µmolSDS
- 753246RuPhos Pd G2 5 µmolSDS
- 756482P(t-Bu)3 Pd G2 5 µmolSDS
recommended
related product
Signal Word
Danger
Hazard Statements
Precautionary Statements
Hazard Classifications
Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Aquatic Acute 1 - Aquatic Chronic 1 - Carc. 1B - Eye Dam. 1 - Repr. 1B - Self-heat. 1 - Skin Corr. 1B - STOT RE 2 Oral - STOT SE 3
Target Organs
Central nervous system, Kidney,Adrenal gland,Testes, Respiratory system
Supplementary Hazards
WGK
WGK 3
Flash Point(F)
-4.0 °F
Flash Point(C)
-20 °C
Regulatory Information
Certificates of Analysis (COA)
Search for Certificates of Analysis (COA) by entering the products Lot/Batch Number. Lot and Batch Numbers can be found on a product’s label following the words ‘Lot’ or ‘Batch’.
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Articles
KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.
Materials Included in your KITALYSIS-24PD-2PK High-Throughput Screening Kit
Preformed catalysts in the kit are stable but become air-sensitive when activated; Schlenk technique aids scale-up.
Preformed catalysts in the kit are stable but become air-sensitive when activated; Schlenk technique aids scale-up.
Protocols
Protocol for the KitAlysis™ Buchwald-Hartwig Amination Reaction Screening Kit
Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
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Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
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