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KITALYSIS-SM

Sigma-Aldrich

KitAlysis™ 高通量 Suzuki-Miyaura 交叉偶联反应筛选试剂盒 - 4 件装

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别名:
Suzuki-Miyaura 交叉偶联
UNSPSC代码:
12352200
NACRES:
NA.22

应用

Suzuki-Miyaura 交叉偶联反应筛选试剂盒。下面的超链接提供了逐步用户指南和可下载的实验 excel 表格。
Suzuki-Miyaura 交联反应筛选试剂盒的逐步指南
可下载的实验 excel 表格

每个试剂盒包含 4 个可定制筛选集，包括以下组件：
  • 6 x 4 预称重催化剂，装在带搅拌棒和盖垫的玻璃瓶内
  • 1 (2 mL) 安培瓶，各含甲苯、THF、正丁醇, DMAc 和 aq.1.5 M K3PO4。
  • 4 个新的 KitAlysis 24 孔反应块置换膜。
  • 4 个带搅拌棒的底物反应瓶。
  • 1 个内部标准品。
通过 TLC-MS，按 本方案监控反应进程

最好配合 KitAlysis 使用台式分析箱 and 24 孔反应块（单独销售）。

特点和优势

  • 由合成化学家设计和测试。
  • 轻松平行运行 24 个微量反应。
  • 含 1 μmol 催化剂、3 等当量碱、0.1 M 浓度进行 10 μmol 反应。
  • 可定制的 Excel 模板，可快速计算，并易于整合到电子实验室笔记本中。

法律信息

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

仅试剂盒组分

产品编号
说明
  • SnapIT Ampule Opener, Regular, for 1-2ml, 5-10ml, 10-15ml ampoules 1 EA

试剂盒组分也可单独购买

产品编号
说明
化学品安全说明书
  • 732117Pd-PEPPSI™-IPent catalyst, ≥95% 5 µmol化学品安全说明书
  • 753009SPhos Pd G2 5 µmol化学品安全说明书
  • 761311cataCXium® A Pd G2 5 µmol化学品安全说明书
  • 763381XPhos Pd G3, 98%, 1:1 MTBE adduct 5 µmol化学品安全说明书
  • 764175P(Cy3) Pd G3, 97% 5 µmol化学品安全说明书
  • 764183APhos Pd G3, 97% 5 µmol化学品安全说明书
  • 900522Toluene, anhydrous, ZerO2®, 99.8% 8 mL化学品安全说明书
  • 900636Tetrahydrofuran, anhydrous, inhibitor-free, ZerO2®, ≥99.9% 8 mL化学品安全说明书
  • 9006391-Butanol, anhydrous, ZerO2®, 99.8% 8 mL化学品安全说明书
  • 900634N,N-Dimethylacetamide, anhydrous, ZerO2®, 99.8% 8 mL化学品安全说明书
  • Degassed Potassium phosphate tribasic solution 8 mL
  • Z118850Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mm 1 EA化学品安全说明书
查看所有结果 (12)

警示用语：

Danger

危险分类

Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Asp. Tox. 1 - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2 - STOT SE 3

靶器官

Central nervous system, Respiratory system

补充剂危害

EUH019

WGK

WGK 3

闪点(°F)

1.4 °F

闪点(°C)

-17 °C

法规信息

易制毒化学品（3类）
危险化学品

分析证书(COA)

输入产品批号来搜索 分析证书(COA) 。批号可以在产品标签上"批“ （Lot或Batch）字后找到。

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在文件库中查找您最近购买产品的文档。

访问文档库

High-Throughput Experimentation in Catalysis and Materials Science.
Gordillo A, et al.
Ullmann's Encyclopedia of Industrial Chemistry (2014)
Karl D Collins et al.
Nature chemistry, 6(10), 859-871 (2014-09-23)
New organic reactivity has often been discovered by happenstance. Several recent research efforts have attempted to leverage this to discover new reactions. In this Review, we attempt to unify reported approaches to reaction discovery on the basis of the practical
Scientist-Led High-Throughput Experimentation (HTE) and Its Utility in Academia and Industry.
Schmink JR, et al.
Aldrichimica Acta, 46, 71-80 (2013)
Spencer D Dreher et al.
Journal of the American Chemical Society, 130(29), 9257-9259 (2008-06-28)
Microscale parallel experimentation was used to discover three catalyst systems capable of coupling secondary organotrifluoroborates with sterically and electronically demanding aryl chlorides and bromides. The ensuing results represent the first comprehensive study of alkylboron coupling to aryl chlorides and, in

商品

Scale-Up Guide: Suzuki-Miyaura Cross-Coupling Reaction

All of the preformed catalysts used in the kit are air and moisture stable complexes in their commercially available form.

KitAlysis™ High-Throughput Screening Platform

KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.

KitAlysis™ Suzuki-Miyaura Cross-Coupling Kit

Tools aid in kit setup for organic chemistry techniques, ensuring ease and success.

KitAlysis High-Throughput Palladium Precatalyst Cross-Coupling Reaction Screening Kit

Materials Included in your KITALYSIS-24PD-2PK High-Throughput Screening Kit

实验方案

Step-by-Step Guide for KitAlysis™ Suzuki-Miyaura Cross-Coupling Reaction Screening Kit

A step-by-step protocol guide for KitAlysis Suzuki-Miyaura Cross-Coupling Reaction Screening Kit.

相关内容

Reaction Design & Optimization

Chemical reaction design and optimization in organic synthesis aims to precisely alter reaction parameters to achieve optimum results in finding pathways to target molecules.

化学反应设计_化学反应优化_催化剂-默克生命科学

化学反应的设计和优化是有机合成研究的重要手段，通过改变反应参数，例如催化剂、反应体系pH值、反应溶剂、温度或时间等来节约成本、提高反应的选择性、产物的收率和纯度等

我们的科学家团队拥有各种研究领域经验，包括生命科学、材料科学、化学合成、色谱、分析及许多其他领域.

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