product line
KitAlysis™
reaction suitability
reaction type: Buchwald-Hartwig Amination
reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Cross Couplings
reagent type: catalyst
core: palladium
storage temp.
room temp
Application
两种溶剂，弱碱（Cs2CO3）
在此处下载实验excel文件
两种溶剂，强碱（NaOt-Bu）
在此处下载实验excel文件
一种溶剂（二恶烷），两种碱
在此处下载实验excel文件
一种溶剂（DMAc），两种碱
在此处下载实验excel文件
每个试剂盒中包含4组筛选，包括以下内容：
每个可定制的筛选套件包含
- 12 X 2每个预称重的催化剂 (1 μmol) 在带有磁性搅拌棒的单个小瓶中
- 2种碱(NaOt-Bu and Cs2CO3)
- 2个装在安瓿瓶中的脱气无水溶剂（二氧六环和DMAc）
- 2 个带有搅拌棒的底物反应瓶
- 1 个内标
- 4个反应遮挡可替换膜
使用KitAlysis效果最佳 B台式插入盒 和 24-孔反应块 （单独销售）。
Features and Benefits
- 由合成化学家设计和测试
- 轻松平行运行 24 个微型反应
- 含 1 μmol 催化剂、3 当量碱、0.1 M 浓度的 10μmol 反应
- 可定制的 Excel 模板，可快速计算，并易于整合到电子实验室笔记本中
General description
Legal Information
signalword
Danger
Hazard Classifications
Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Aquatic Acute 1 - Aquatic Chronic 1 - Carc. 1B - Eye Dam. 1 - Repr. 1B - Self-heat. 1 - Skin Corr. 1B - STOT RE 2 Oral - STOT SE 3
target_organs
Central nervous system, Kidney,Adrenal gland,Testes, Respiratory system
supp_hazards
存储类别
4.2 - Pyrophoric and self-heating hazardous materials
flash_point_f
-4.0 °F - closed cup
flash_point_c
-20 °C - closed cup
法规信息
商品
All contents in the foil bag are weighed, plated, packed, and sealed in a glove box under nitrogen.
KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.
Preformed catalysts in the kit are stable but become air-sensitive when activated; Schlenk technique aids scale-up.
Materials Included in your KITALYSIS-24PD-2PK High-Throughput Screening Kit
实验方案
Catalyst screening kits, KitAlysis™, and TLC-MS analysis enable high-throughput synthesis and analysis for efficient reactions.
Protocol for the KitAlysis™ Buchwald-Hartwig Amination Reaction Screening Kit
Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
KitAlysis™ Cu C-N (Buchwald-Hartwig) cross-coupling high-throughput screening kit. Detailed Set-Up User Guide and a downloadable excel file for calculations.
相关内容
化学反应的设计和优化是有机合成研究的重要手段，通过改变反应参数，例如催化剂、反应体系pH值、反应溶剂、温度或时间等来节约成本、提高反应的选择性、产物的收率和纯度等
Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
我们的科学家团队拥有各种研究领域经验，包括生命科学、材料科学、化学合成、色谱、分析及许多其他领域.
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