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sample preparation	SPE (Solid Phase Extraction)
sample/matrix	water spiked with phenol compounds
SPE tube/cartridge	Supelclean ENVI-Chrom P, 250 mg/6 mL (57225-U)
condition	6 mL methyl t-butyl or ethyl acetate; 6 mL acetonitrile. Equilibrate with 6 mL DI water
sample addition	100 mL water sample.
drying	10 min using vacuum
elution	5 mL methyl t-butyl ether acetate dropwise allowing initial 2 mL to soak in SPE bed
column	5% Phenyl Polysiloxane, 15 m x 0.53 mm I.D., 0.50 µM (Supelco equivalent, Equity-5, 28252-U)
oven	65 °C, 10 °C/min to 185 °C (1 min), 20 °C/min to 275 °C (5 min)
carrier gas	helium
injection	1 µL, splitless (45 sec hold)
detector	FID, 300 °C

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Categories	Analytical Chromatography, SPE Applications, GC Applications, Phenols & Semivolatiles in water, Phenols
Featured Industry	Chemicals and Industrial Polymers \r\nEnvironmental \r\nFood and Beverages
Legal Information	Supelclean is a trademark of Sigma-Aldrich Co. LLC
Other Notes	Complementary products: \r\nSyringes \r\nVials \r\nGas Purification and Gas Management \r\nInlet Liners, Glass Wool, and Specialized Hand Tools \r\nSepta and Specialized Hand Tools \r\nColumn Ferrules, Nuts, and Specialized Hand Tools
suitability	application for GC, application for SPE

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Analyte

\r\n

2,3,4,6-Tetrachlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2-Bromophenol
2-Chlorophenol
2-Methylphenol
2-Nitrophenol
3-Methylphenol
4-Chloro-3-methylphenol
4-Nitrophenol
Pentachlorophenol
Phenol

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