Skip to Content
Merck
CN
  • Vine-shoot waste aqueous extracts for re-use in agriculture obtained by different extraction techniques: phenolic, volatile, and mineral compounds.

Vine-shoot waste aqueous extracts for re-use in agriculture obtained by different extraction techniques: phenolic, volatile, and mineral compounds.

Journal of agricultural and food chemistry (2014-10-23)
Rosario Sánchez-Gómez, Amaya Zalacain, Gonzalo L Alonso, M Rosario Salinas
ABSTRACT

Vine-shoots are an important waste in all viticulture areas that should be re-used with innovative applications. The aim of this work was to produce Airén waste vine-shoot aqueous extracts by four solid-liquid extraction techniques such as conventional solid-liquid extraction (CSLE), solid-liquid dynamic extraction (SLDE-Naviglio), microwave extraction (ME), and pressurized solvent extraction (PSE). Their chemical composition was studied in terms of phenolic, volatile, and mineral compounds. The highest concentrated extracts corresponded to CSLE and SLDE-Naviglio, independent of the conditions tested. The CSLE extracts had the highest flavanols, phenolic acids, and stilbenes contents. The volatile composition, quantified for first time in this work, shows that furanic compounds were the most abundant. All extracts showed an interesting mineral content, which may be assimilated by plants. These results show the agricultural potential of Airén vine-shoot waste aqueous extracts to be used as grape biostimulants and/or foliar fertilizer.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
Decanoic acid, ≥98.0%
Sigma-Aldrich
Guaiacol, oxidation indicator
Supelco
Decanoic acid, analytical standard
Supelco
Benzaldehyde, analytical standard
Sigma-Aldrich
Benzaldehyde, puriss. p.a., ≥99.0% (GC)
Sigma-Aldrich
Hexanoic acid, purum, ≥98.0% (GC)
Sigma-Aldrich
Nonyl alcohol, ≥98%, FCC
Sigma-Aldrich
5-Methylfurfural, ReagentPlus®, 99%
Sigma-Aldrich
Vanillin, ReagentPlus®, 99%
Sigma-Aldrich
Vanillin, natural, ≥97%, FCC, FG
Sigma-Aldrich
Hexanoic acid, ≥98%, FCC, FG
Sigma-Aldrich
Furfural, ACS reagent, 99%
Sigma-Aldrich
Linalool, 97%
Sigma-Aldrich
Vanillin, tested according to Ph. Eur.
Supelco
Hexanoic acid, analytical standard
Benzaldehyde, European Pharmacopoeia (EP) Reference Standard
Supelco
5-Methylfurfural, analytical standard
Supelco
Benzaldehyde, Pharmaceutical Secondary Standard; Certified Reference Material
Supelco
Vanillin, certified reference material, TraceCERT®, Manufactured by: Sigma-Aldrich Production GmbH, Switzerland
Guaiacol, European Pharmacopoeia (EP) Reference Standard
Supelco
Linalool, analytical standard
Supelco
Vanillin melting point standard, Pharmaceutical Secondary Standard; Certified Reference Material
Supelco
Guaiacol, Pharmaceutical Secondary Standard; Certified Reference Material
USP
Vanillin Melting Point Standard, United States Pharmacopeia (USP) Reference Standard
Sigma-Aldrich
Vanillin, ≥97%, FCC, FG
Sigma-Aldrich
5-Methylfurfural, ≥98%, FG
Sigma-Aldrich
Hexanoic acid, ≥99%
Sigma-Aldrich
Benzaldehyde, purified by redistillation, ≥99.5%
Sigma-Aldrich
Decanoic acid, natural, ≥98%, FCC, FG
Sigma-Aldrich
Decanoic acid, ≥99.5%, FCC, FG