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G005933

GC Analysis of Volatiles in Purple Nitrile Gloves on SPB®-HAP after Collection/Desorption using Carbotrap® 300 Tube

suitable for GC, application for air monitoring

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technique(s)

gas chromatography (GC): suitable

test parameters

sample/matrix: 0.5 g purple nitrile glove
thermal desorption tube: Carbotrap® 300 Glass-Fritted Thermal Desorption Tube, 1/4 in O.D. x 3.5 in L (30141-U)
desorption process: 350 °C with 10 min hold
transfer line/valve temp.: 180 °C
column: SPB®-HAP, 60 m x 0.32 mm I.D., 4 μm (25020-U)
oven: 40 °C (3 min), 12 °C/min to 200 °C (20 min)
detector: MSD
MSD interface: 210 °C
carrier gas: helium
dry purge: 15 min

suitability

application for air monitoring

application(s)

air monitoring
industrial hygiene

General description

Qualitative volatile headspace outgassing from purple nitrile gloves using the ATIS system with analysis by thermal desorption.

Legal Information

Carbotrap is a registered trademark of Merck KGaA, Darmstadt, Germany
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyte

Description
    Carbon disulfide
    Methacrylic acid
    Diethylcyanamide
    N,N-Diethylformamide
    6-Methyl-5-hepten-2-one
    4-Cyanocyclohexene
    Naphthalene

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