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796-0086

HPLC Analysis of PAHs in Water on SUPELCOSIL™ LC-PAH after SPME using 100 μm PDMS Fiber

application for SPME, application for HPLC

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technique(s)

HPLC: suitable
solid phase microextraction (SPME): suitable

test parameters

sample/matrix: 5 μL PAH mix (Cat. No. 4-8743) in 5 mL water
SPME fiber: polydimethylsiloxane, 100 μm (57301)
extraction: immersion, 30 min (rapid stirring)
desorption process: static, 200 μL acetonitrile:water, 40:60, 2 min
column: SUPELCOSIL LC-PAH, 15 cm × 4.6 mm I.D., 5 μm particles (58318)
gradient: 0 min - 50% A; 5 min - 50% A; 30 min - 100% A; 45 min - 100% A
flow rate: 0-2 min: 0.2 mL/min 2-45 min: 1.0 mL/min
mobile phase: [A] acetonitrile:[B] water
detector: UV, 254 nm

suitability

application for HPLC
application for SPME

application(s)

environmental

Legal Information

SUPELCOSIL is a trademark of Sigma-Aldrich Co. LLC

Analyte

Description
    Chrysene
    Naphthalene
    Benzo[b]fluoranthene
    Phenanthrene
    Indeno[1,2,3-cd]pyrene
    Benzo[a]pyrene
    Fluoranthene
    Anthracene
    Dibenz[a,h]anthracene
    Pyrene
    Acenaphthylene
    Benzo[k]fluoranthene
    Acenaphthene
    Fluorene
    Benz[a]anthracene
    See All (15)

SPME fiber

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Description
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analytical column

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