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52739-U

Supelco

Discovery® DSC-WCX SPE Tube

bed wt. 100 mg, volume 1 mL, pk of 108

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UNSPSC Code:
41115712
NACRES:
NB.21

material

polypropylene tube

Quality Level

composition

bed wt., 100 mg

packaging

pk of 108

technique(s)

solid phase extraction (SPE): suitable

surface area

480 m2/g

volume

1 mL

matrix

Silica gel base material (irregularly shaped, acid washed)

matrix active group

carboxypropyl bonding

particle size

50 μm

pore size

0.9 mL/g pore volume
70 Å pore diameter

capacity

0.15 meq/g total capacity

application(s)

food and beverages

separation technique

ion exchange

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General description

Retention Mechanism: Cation exchange
Sample Matrix Compatibility: Organic or aqueous solutions

  • A polymerically bonded, ethylenediamine triacetic acid phase with a pKa of 4.8
  • Counter ion is Na+
  • Ion exchange capacity is ∼ 0.15 meq/g
  • Carries a negative charge at pH 6.8 or above
  • A pH of 2.8 or below neutralizes this phase for easier elution of strong cationic analytes that are neutralized only at extreme basic conditions
  • Typically used when dealing with very strong cationic (high pKa) compounds that may be irreversibly retained on strong cation exchangers

Legal Information

Discovery is a registered trademark of Merck KGaA, Darmstadt, Germany

Pictograms

CorrosionExclamation mark

Signal Word

Danger

Hazard Statements

Hazard Classifications

Aquatic Chronic 3 - Eye Dam. 1 - Skin Sens. 1

WGK

WGK 3


Certificates of Analysis (COA)

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Articles

SPE retention mechanism in this case is based on the electrostatic attraction of charged functional groups of the analyte(s) to oppositely charged functional groups on the sorbent.

Protocols

Normal-phase SPE separates analytes based on polar interaction with sorbents in diverse sample matrices.

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