52689-U
Discovery® DSC-SCX SPE Tube
bed wt. 1 g, volume 6 mL, pk of 30
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material
polypropylene tube
Quality Level
composition
bed wt., 1 g
packaging
pk of 30
technique(s)
solid phase extraction (SPE): suitable
surface area
480 m2/g
volume
6 mL
matrix
Silica gel base material (irregularly shaped, acid washed)
matrix active group
sulfonic acid bonding
particle size
50 μm
pore size
0.9 mL/g pore volume
70 Å pore diameter
capacity
0.8 meq/g total capacity
application(s)
food and beverages
separation technique
ion exchange
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General description
Sample Matrix Compatibility: Organic or aqueous solutions
- A polymerically bonded, benzene sulfonic acid functional group, pKa (< 1.0)
- Counter ion is H+
- Silica support allows for use with very organic solvents (no shrinking/swelling)
- Excellent capacity (0.8 meq/g) for cleaning up solution phase combinatorial chemistry reactions (removing target molecules from reaction by-products and excess reagents)
- The presence of the benzene ring offers some mixed-mode capabilities (hydrophobic interactions) that should be considered when extracting cations from aqueous matrices
Legal Information
Signal Word
Danger
Hazard Statements
Precautionary Statements
Hazard Classifications
Aquatic Chronic 2 - Eye Dam. 1 - Flam. Sol. 1 - Skin Corr. 1A - Skin Sens. 1
WGK
WGK 3
Flash Point(F)
Not applicable
Flash Point(C)
Not applicable
Certificates of Analysis (COA)
Search for Certificates of Analysis (COA) by entering the products Lot/Batch Number. Lot and Batch Numbers can be found on a product’s label following the words ‘Lot’ or ‘Batch’.
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Articles
SPE retention mechanism in this case is based on the electrostatic attraction of charged functional groups of the analyte(s) to oppositely charged functional groups on the sorbent.
Protocols
Melamine was extracted from milk using Supelco® Discovery® DSC-SCX SPE tubes. Analysis was performed by HPLC, using an Ascentis® Express HILIC column.
Normal-phase SPE separates analytes based on polar interaction with sorbents in diverse sample matrices.
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