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Discovery® DPA-6S SPE Bulk Packing

pkg of 50 g

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UNSPSC Code:
41115712
NACRES:
NB.21

packaging

pkg of 50 g

technique(s)

solid phase extraction (SPE): suitable

matrix active group

amide, poly- phase

application(s)

food and beverages

separation technique

reversed phase

General description

Retention Mechanism: Reversed-phase
Sample Matrix Compatibility: Aqueous or methanolic solutions

  • Polyamide Resin: Particle Size: 50-160μm, Surf pH: 4.5-7.5, Density: 0.2-0.3 cm3/g, Water Content: < 5 %
  • Used to adsorb polar compounds (-OH groups, esp. phenolic compounds) from aqueous or methanolic solutions under the reversed-phase mechanism through strong hydrogen bonding between compound hydroxyl groups and amide groups of the resin
  • Useful for extracting tannins, chlorophyll, humic acid, pharmacologically active terpenoids, flavanoids, gallic acid, catechol A, protocatechuic acid, and phloroglucinol
  • Also useful for extracting aromatic carboxylic acids and nitroaromatic compounds
  • Irreversibly retains quinones

Application

Discovery® DPA-6S SPE Bulk Packing may be used as a sorbent for dispersive soilid phase extraction followed by liquid chromatography and gas chromatographic determination of acrylamide in various food matrices.

Legal Information

Discovery is a registered trademark of Merck KGaA, Darmstadt, Germany

WGK

WGK 3

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable

Personal Protective Equipment

dust mask type N95 (US), Eyeshields, Gloves

Certificates of Analysis (COA)

Search for Certificates of Analysis (COA) by entering the products Lot/Batch Number. Lot and Batch Numbers can be found on a product’s label following the words ‘Lot’ or ‘Batch’.

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Rapid sample preparation method for LC- MS/MS or GC- MS analysis of acrylamide in various food matrices
Mastovska K and Lehotay JS
Journal of Agricultural and Food Chemistry, 54(19), 7001-7008 (2006)
Takayuki Asada et al.
Journal of chromatography. A, 1351, 21-28 (2014-06-04)
Isolation techniques for anthocyanidin 3,5-diglucosides and their derivatives from three types of supramolecular pigments were newly developed using two SPE (Discovery DPA-6S and DSC-SCX) cartridges. Initially, malonylawobanin from commelinin supramolecular complex yielded 79.5% with 85.7% purity using DPA-6S, while DSC-SCX
Takayuki Asada et al.
Food chemistry, 166, 10-16 (2014-07-24)
An aluminium complex of crude Delaware grape anthocyanins, bearing an ortho-dihydroxyl group on the B ring and/or a p-coumaroyl group as an ester with flavocommelin, was formed and isolated by ethanol precipitation. Using a Discovery DPA-6S short column, selected anthocyanins

Articles

Solid Phase Extraction: Reversed-Phase Methodology

Reversed-phase interaction will retain most molecules with hydrophobic character; it is very useful for extracting analytes that are very diverse in structure within the same sample.

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