52633-U
Discovery® DPA-6S SPE Bulk Packing
pkg of 50 g
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About This Item
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packaging
pkg of 50 g
technique(s)
solid phase extraction (SPE): suitable
matrix active group
amide, poly- phase
application(s)
food and beverages
separation technique
reversed phase
General description
Retention Mechanism: Reversed-phase
Sample Matrix Compatibility: Aqueous or methanolic solutions
Sample Matrix Compatibility: Aqueous or methanolic solutions
- Polyamide Resin: Particle Size: 50-160μm, Surf pH: 4.5-7.5, Density: 0.2-0.3 cm3/g, Water Content: < 5 %
- Used to adsorb polar compounds (-OH groups, esp. phenolic compounds) from aqueous or methanolic solutions under the reversed-phase mechanism through strong hydrogen bonding between compound hydroxyl groups and amide groups of the resin
- Useful for extracting tannins, chlorophyll, humic acid, pharmacologically active terpenoids, flavanoids, gallic acid, catechol A, protocatechuic acid, and phloroglucinol
- Also useful for extracting aromatic carboxylic acids and nitroaromatic compounds
- Irreversibly retains quinones
Application
Discovery® DPA-6S SPE Bulk Packing may be used as a sorbent for dispersive soilid phase extraction followed by liquid chromatography and gas chromatographic determination of acrylamide in various food matrices.
Legal Information
Discovery is a registered trademark of Merck KGaA, Darmstadt, Germany
Storage Class Code
11 - Combustible Solids
WGK
WGK 3
Flash Point(F)
Not applicable
Flash Point(C)
Not applicable
Personal Protective Equipment
dust mask type N95 (US), Eyeshields, Gloves
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Rapid sample preparation method for LC- MS/MS or GC- MS analysis of acrylamide in various food matrices
Journal of Agricultural and Food Chemistry, 54(19), 7001-7008 (2006)
Food chemistry, 166, 10-16 (2014-07-24)
An aluminium complex of crude Delaware grape anthocyanins, bearing an ortho-dihydroxyl group on the B ring and/or a p-coumaroyl group as an ester with flavocommelin, was formed and isolated by ethanol precipitation. Using a Discovery DPA-6S short column, selected anthocyanins
Journal of chromatography. A, 1351, 21-28 (2014-06-04)
Isolation techniques for anthocyanidin 3,5-diglucosides and their derivatives from three types of supramolecular pigments were newly developed using two SPE (Discovery DPA-6S and DSC-SCX) cartridges. Initially, malonylawobanin from commelinin supramolecular complex yielded 79.5% with 85.7% purity using DPA-6S, while DSC-SCX
Articles
Reversed-phase interaction will retain most molecules with hydrophobic character; it is very useful for extracting analytes that are very diverse in structure within the same sample.
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