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Supelco

SPB®-1701

column L × I.D. 30 m × 0.32, df 0.25 μm

Synonym(s):

SPB-1701 30M .25UM .32MM

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About This Item

UNSPSC Code:
12000000

material

fused silica

description

GC Capillary Column

Beta value

320

df

0.25 μm

technique(s)

gas chromatography (GC): suitable

column L × I.D.

30 m × 0.32

matrix active group

bonded; poly(14% cyanopropylphenyl/86% dimethyl siloxane) phase

McReynolds constant

67, 170, 153, 228, 171

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General description

A leader in special purpose capillary columns, Supelco, offers the broadest range of bonded cyanopropyl- functional phases in the industry. The SPB-1701 is an intermediate polarity column that generates unique elution order characteristics relative to typical polymethyl siloxane phases with some degree of phenyl group substitution. This column is suitable for popular applications such as Alditol Acetates and Pesticides. Proprietary Supelco cross-linking technology found in the stationary phase of SPB-1701 allows for reproducible quantitation of analytes with mimimum sensitivity degradation due to phase bleed.

This column meets USP G46 requirements.
Intermediate polarity SPB®-1701 columns have a mixed functionality which provides unique elution order characteristics, relative to the phenyl-containing silicone phases.

Application

SPB®-1701 is suitable to be used in gas chromatograph-thermal energy analyzer, used for the for the analysis of metabolites of the tobacco-specific lung carcinogen 4-(methylnitrosamino)-1-(3-pyridyl)-1-butanone (NNK) in human urine.

Chem/Phys Resistance

Temp. Limits: subambient to 280°C
McReynolds Nos.: X′ y′ z′ u′ s′ = 67 170 153 228 171

Legal Information

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

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Steven G Carmella et al.
Cancer epidemiology, biomarkers & prevention : a publication of the American Association for Cancer Research, cosponsored by the American Society of Preventive Oncology, 12(11 Pt 1), 1257-1261 (2003-12-04)
A new method was developed for the analysis of metabolites of the tobacco-specific lung carcinogen 4-(methylnitrosamino)-1-(3-pyridyl)-1-butanone (NNK) in human urine. The metabolites are 4-(methylnitrosamino)-1-(3-pyridyl)-1-butanol (NNAL) and its glucuronides (NNAL-O-Gluc and NNAL-N-Gluc). The sum of these metabolites, total NNAL, was measured

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