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24010

Supelco

SP®-2250 Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.20 μm

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UNSPSC Code:
41115710
eCl@ss:
32119290

material

fused silica

Agency

meets requirements for USP G3

parameter

0-250 °C temperature (isothermal or programmed)

Beta value

313

df

0.20 μm

technique(s)

gas chromatography (GC): suitable

L × I.D.

30 m × 0.25 mm

matrix active group

Non-bonded; poly(50% phenyl/50% methyl siloxane) phase

column type

capillary intermediate polar

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General description

Application: The SP-2250 column is a non-bonded 50% phenyl polymer. It is highly effective for the analysis of polar compounds.
USP Code: This column meets USP G3 requirements.
Phase:
  • Non-bonded
  • Poly(50% phenyl/50% methyl siloxane)
Temp. Limits:
  • 0 °C to 250 °C (isothermal or programmed)

Application

Capillary column coated with SP®-2250 (methyl silicone-phenyl silicone, 1:1) stationary phase may be used in gas chromatographic analysis of azaarenes (benzacridines and dibenzacridines).

Other Notes

We offer a variety of chromatography accessories including analytical syringes

Legal Information

SP is a registered trademark of Sigma-Aldrich Co. LLC

Regulatory Information

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K Nakamura et al.
Investigative ophthalmology & visual science, 31(10), 2059-2069 (1990-10-01)
Silicone oil (SiO) and fluorosilicone oil (FSiO) are useful in difficult cases of retinal detachment surgery. Unidentified low-molecular-weight components (LMWC) and residual catalysts in SiO and FSiO have been implicated in the adverse reactions of the oils in the eye.
H B Hucker et al.
Journal of pharmaceutical sciences, 72(9), 1069-1070 (1983-09-01)
A method for the determination of cyproheptadine in plasma and urine was developed using the N -ethyl homologue as an internal standard. After extraction of the drug from an alkalinized sample into petroleum ether-isoamyl alcohol, back-extraction into 0.1 N HCl
D J Greenblatt et al.
Anesthesiology, 55(2), 176-179 (1981-08-01)
Plasma midazolam concentrations following single therapeutic doses can be quantitated using electron-capture gas-liquid chromatography. After addition of a benzodiazepine analogue as an internal standard, samples are extracted with benzeneisoamyl alcohol (98.5:1.5). The organic extract is evaporated to dryness, reconstituted, and
W Löscher
Therapeutic drug monitoring, 4(3), 315-318 (1982-01-01)
A rapid method was developed for the determination of diazepam, desmethyldiazepam, oxazepam, and 3-hydroxydiazepam (temazepam) in human plasma using electron capture gas chromatography. Following a single extraction with benzene from 0.2 ml plasma, diazepam and its metabolites were quantitated on
O W Lau et al.
Methods and findings in experimental and clinical pharmacology, 13(7), 475-481 (1991-09-01)
A gas-liquid chromatographic method was developed for the simultaneous assay of six local anesthetics, including amethocaine, bupivacaine, etidocaine, lignocaine, mepivacaine and prilocaine, in biological samples. These drugs and internal standard (clomipramine) in basified samples were extracted into 5 ml n-hexane

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