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32759

Supelco

Patulin

reference material

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Synonym(s):
4-Hydroxy-4H-furo[3,2-c]pyran-2(6H)-one
Empirical Formula (Hill Notation):
C7H6O4
CAS Number:
149-29-1
Molecular Weight:
154.12
Beilstein:
149675
EC Number:
205-735-2
MDL number:
MFCD00005858
UNSPSC Code:
85151701
PubChem Substance ID:
329754321
NACRES:
NA.24

grade

analytical standard
reference material

shelf life

limited shelf life, expiry date on the label

technique(s)

HPLC: suitable
gas chromatography (GC): suitable

application(s)

cleaning products
cosmetics
food and beverages
personal care

format

neat

storage temp.

−20°C

SMILES string

OC1OCC=C2OC(=O)C=C12

InChI

1S/C7H6O4/c8-6-3-4-5(11-6)1-2-10-7(4)9/h1,3,7,9H,2H2

InChI key

ZRWPUFFVAOMMNM-UHFFFAOYSA-N

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General description

Patulin (PAT) is a mycotoxin of the polyketide lactone type, usually produced by species of the Penicillium, Aspergillus and Byssochlamys genera.

Application

PAT may be used as a reference standard for the determination of patulin in:
  • Fruit-based products by QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe) method and solid phase extraction (SPE) followed by analysis using ultra-high performance liquid chromatography combined with electrospray ionization tandem mass spectrometry (UHPLC-ESI-MS/MS).
  • Apple juice samples by single drop liquid-liquid-liquid microextraction (SD-LLLME) followed by LC-MS/MS analysis.
  • Model food matrices by “dilute and shoot” LC-MS/MS.
  • Dairy products by QuEChERS procedure and UHPLC-ESI quadrupole orbitrap (Q-Orbitrap) mass spectrometry.

Refer to the product′s Certificate of Analysis for more information on a suitable instrument technique. Contact Technical Service for further support.

Pictograms

Skull and crossbones
GHS06

Signal Word

Danger

Hazard Statements

H300,H315

Hazard Classifications

Acute Tox. 2 Oral - Skin Irrit. 2

WGK

WGK 3

Personal Protective Equipment

dust mask type N95 (US), Eyeshields, Gloves

Regulatory Information

监管及禁止进口产品

Certificates of Analysis (COA)

Search for Certificates of Analysis (COA) by entering the products Lot/Batch Number. Lot and Batch Numbers can be found on a product’s label following the words ‘Lot’ or ‘Batch’.

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Monitoring survey of patulin in a variety of fruit-based products using a sensitive UHPLC-MS/MS analytical procedure.
Vaclavikova M, et al.
Food Control, 47, 577-584 (2015)
Determination of patulin in apple juice by single-drop liquid-liquid-liquid microextraction coupled with liquid chromatography-mass spectrometry.
Li X, et al.
Food Chemistry, 257, 1-6 (2018)
Multi-mycotoxin analysis in dairy products by liquid chromatography coupled to quadrupole orbitrap mass spectrometry.
Jia W, et al.
Journal of Chromatography A, 1345, 107-114 (2014)
Molecularly imprinted polymer for extraction of patulin in apple juice samples.
Anene A, et al.
Food Control, 70, 90-95 (2016)
Optimization and validation of a quantitative liquid chromatography-tandem mass spectrometric method covering 295 bacterial and fungal metabolites including all regulated mycotoxins in four model food matrices.
Malachova A, et al.
Journal of Chromatography A, 1362, 145-156 (2014)
View All Related Papers

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