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Merck
CN

23186

Fmoc chloride

≥99.0%, for HPLC derivatization, LiChropur™

Synonym(s):

9-Fluorenylmethoxycarbonyl chloride, 9-Fluorenylmethyl chloroformate, Fmoc-Cl

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About This Item

Empirical Formula (Hill Notation):
C15H11ClO2
CAS Number:
28920-43-6
Molecular Weight:
258.70
NACRES:
NA.22
PubChem Substance ID:
329752393
UNSPSC Code:
41115710
EC Number:
249-313-6
MDL number:
MFCD00001138
Beilstein/REAXYS Number:
2279177

Key Documents

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Product Name

Fmoc chloride, derivatization grade (HPLC), LiChropur™, ≥99.0% (HPLC)

InChI key

IRXSLJNXXZKURP-UHFFFAOYSA-N

InChI

1S/C15H11ClO2/c16-15(17)18-9-14-12-7-3-1-5-10(12)11-6-2-4-8-13(11)14/h1-8,14H,9H2

SMILES string

ClC(=O)OCC1c2ccccc2-c3ccccc13

grade

derivatization grade (HPLC)

assay

≥99.0% (HPLC)

form

solid

quality

LiChropur™

technique(s)

HPLC: suitable

mp

61-64 °C
62-64 °C (lit.)

storage temp.

2-8°C

Quality Level

100

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Application

Fmoc chloride may be used as derivatizing reagent in pre-column derivatization of the biogenic amines, resolved using HPLC technique.
Reagent for derivatizing amino acids for HPLC amino acid analysis and for preparing N-Fmoc amino acids for solid-phase peptide synthesis.

General description

Fmoc chloride is a derivatizing agent.

Other Notes

Discover LiChropur reagents ideal for HPLC or LC-MS analysis
Reagent for precolumn derivatization of amines for HPLC and fluorescent detection (abs.: 265 nm, em.: 315 nm); Used for capillary electrophoresis

Legal Information

LiChropur is a trademark of Merck KGaA, Darmstadt, Germany

pictograms

Corrosion
GHS05

signalword

Danger

hcodes

H314

Hazard Classifications

Eye Dam. 1 - Skin Corr. 1B

supp_hazards

EUH029

Storage Class

8A - Combustible corrosive hazardous materials

wgk

WGK 3

flash_point_f

Not applicable

flash_point_c

Not applicable

ppe

Eyeshields, Faceshields, Gloves, type P3 (EN 143) respirator cartridges

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Certificates of Analysis (COA)

Lot/Batch Number
BCCM6531
BCCM7018
BCCM2032
BCCK2058
BCCK2354

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J. Kirschbaum et al.
Journal of Chromatography A, 661, 193-193 (1994)
J.V. Sancho et al.
Journal of Chromatography A, 678, 59-59 (1994)
K C Chan et al.
Journal of chromatography. A, 653(1), 93-97 (1993-10-29)
Laser-induced fluorescence (LIF) was applied to the detection of 9-fluorenylmethyl chloroformate (FMOC-Cl) derivatized amino acids separated by capillary electrophoresis. Fluorescence excitation was provided by a pulsed, KrF laser operating at 248 nm. A limit of detection of 5 x 10(-10)
S. Einarsson et al.
Analytical Chemistry, 58, 1638-1638 (1986)
Xuezheng Song et al.
Analytical biochemistry, 395(2), 151-160 (2009-08-25)
Glycan microarray technology has become a successful tool for studying protein-carbohydrate interactions, but a limitation has been the laborious synthesis of glycan structures by enzymatic and chemical methods. Here we describe a new method to generate quantifiable glycan libraries from
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