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Assay
97%
form
solid
mp
200-204 °C
SMILES string
OC(=O)c1ccc(c(Br)c1)[N+]([O-])=O
InChI
1S/C7H4BrNO4/c8-5-3-4(7(10)11)1-2-6(5)9(12)13/h1-3H,(H,10,11)
InChI key
KKPPNEJUUOQRLE-UHFFFAOYSA-N
Application
Substrate linked to a solid support via the carboxyl group which is used in a Bartoli synthesis of indoles.
Signal Word
Warning
Hazard Statements
Precautionary Statements
Hazard Classifications
Acute Tox. 4 Oral
WGK
WGK 3
Flash Point(F)
Not applicable
Flash Point(C)
Not applicable
Personal Protective Equipment
dust mask type N95 (US), Eyeshields, Gloves
Regulatory Information
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Organic letters, 5(16), 2829-2832 (2003-08-02)
[reaction: see text] Bartoli indole synthesis has been performed for the first time on solid supports. Starting from Merrifield resin, immobilization of five nitro benzoic acids was performed. Addition of four different alkenyl Grignard reagents and basic cleavage leads to
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