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Key Documents

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Safety Information

569534

Sigma-Aldrich

Methanol-d4

anhydrous, ≥99.8 atom % D

Synonym(s):

Methyl-d3 alcohol d, Tetradeuteromethanol

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CN¥5,551.31

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100 μL
CN¥5,551.31

About This Item

Linear Formula:
CD3OD
CAS Number:
811-98-3
Molecular Weight:
36.07
Beilstein:
1733278
EC Number:
212-378-6
MDL number:
MFCD00044637
UNSPSC Code:
12352104
PubChem Substance ID:
329758251
NACRES:
NA.21

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grade

anhydrous

Quality Level

200

isotopic purity

≥99.8 atom % D

Assay

≥99% (CP)

form

liquid

expl. lim.

5.5-36.5 % (lit.)

technique(s)

NMR: suitable

impurities

≤0.005% water
water

refractive index

n20/D 1.326 (lit.)

bp

65.4 °C (lit.)

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antibody form

affinity isolated antibody

antibody form

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antibody form

affinity isolated antibody

antibody form

affinity isolated antibody

Quality Level

100

Quality Level

100

Quality Level

100

Quality Level

100

biological source

rabbit

biological source

rabbit

biological source

rabbit

biological source

rabbit

product line

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product line

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product line

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species reactivity

human

species reactivity

human

species reactivity

human

species reactivity

human

General description

Methanol-d4 (CD3OD) is a deuterated NMR solvent useful in NMR-based research and analyses. Absolute infrared absorption intensities of CD3OD have been reported between 8000 and 350cm-1.[1]

Application

Methanol-d4 may be used as a solvent to analyze the rate of exchange of methoxyl group in camphor and norcamphor dimethyl ketals.[2]

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accessory

Product No.
Description
Pricing

Signal Word

Danger

Hazard Classifications

Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Flam. Liq. 2 - STOT SE 1

Target Organs

Eyes,Central nervous system

Storage Class Code

3 - Flammable liquids

WGK

WGK 2

Flash Point(F)

49.5 °F - closed cup

Flash Point(C)

9.7 °C - closed cup

Regulatory Information

危险化学品
美国出口管控1C298产品
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    Lot/Batch Number
    MBBD8627
    MBBC4660
    MBBC1405
    MBBB9118V
    MBBB3880V

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    Infrared intensities of liquids. XVII. Infrared refractive indices from 8000 to 350 cm-1, absolute integrated absorption intensities, transition moments, and dipole moment derivatives of methan-d3-ol and methanol-d4 at 25?C.
    Bertie JE and Zhang SL.
    J. Chem. Phys. , 101(10), 8364-8379 (1994)
    The Rates of Methoxyl Exchange of Camphor and Norcamphor Dimethyl Ketals in Methanol-d4.
    Traylor TG and Perrin CL.
    Journal of the American Chemical Society, 88(21), 4934-4942 (1966)
    Cheng-Kun Lin et al.
    Organic & biomolecular chemistry, 13(7), 2100-2107 (2014-12-20)
    A straightforward synthesis of novel, 2-heterocyclyl polyhydroxylated pyrrolidines is described. Stereocontrolled additions of nucleophiles to cyclic nitrones generated the corresponding 2,3-trans adducts, allowing the synthesis of the corresponding pyrrolidines via key intermediates bearing an alkyne and a nitrile oxide. Three
    Jon Kapla et al.
    Physical chemistry chemical physics : PCCP, 17(34), 22438-22447 (2015-08-08)
    The disaccharide trehalose (TRH) strongly affects the physical properties of lipid bilayers. We investigate interactions between lipid membranes formed by 1,2-dimyristoyl-sn-glycero-3-phosphocholine (DMPC) and TRH using NMR spectroscopy and molecular dynamics (MD) computer simulations. We compare dipolar couplings derived from DMPC/TRH
    William L Scott et al.
    Journal of combinatorial chemistry, 11(1), 34-43 (2008-12-25)
    For the successful implementation of Distributed Drug Discovery (D(3)) (outlined in the accompanying Perspective), students, in the course of their educational laboratories, must be able to reproducibly make new, high quality, molecules with potential for biological activity. This article reports
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