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Merck
CN

536490

2-tert-Butylimino-2-diethylamino-1,3-dimethylperhydro-1,3,2-diazaphosphorine, polymer-bound

200-400 mesh, extent of labeling: 2.0-2.5 mmol/g loading, 1 % cross-linked

Synonym(s):

BEMP resin

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About This Item

UNSPSC Code:
12352128
PubChem Substance ID:
24878163
NACRES:
NA.22
MDL number:
MFCD03095934

Key Documents

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Product Name

2-tert-Butylimino-2-diethylamino-1,3-dimethylperhydro-1,3,2-diazaphosphorine, polymer-bound, 200-400 mesh, extent of labeling: 2.0-2.5 mmol/g loading, 1 % cross-linked

InChI key

ACRRVYBBQUZACX-UHFFFAOYSA-N

SMILES string

C=Cc1ccccc1.C=Cc2ccc(C=C)cc2.CCN(CC)P3(=NC(C)(C)C)N(C)CCCN3Cc4ccccc4

crosslinking

1 % cross-linked

reaction suitability

reaction type: solution phase peptide synthesis
reactivity: proton reactive

extent of labeling

2.0-2.5 mmol/g loading

particle size

200-400 mesh

Quality Level

100

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Related Categories

Application

Phosphazene Bases: a Family of Extremely Strong, Non-Ionic, Non-Charged Nitrogen–Bases
Polymer-supported base used for deprotonation and N-alkylation of weakly acidic heterocycles.

pictograms

Corrosion
GHS05

signalword

Danger

hcodes

H314

Hazard Classifications

Skin Corr. 1B

Storage Class

8A - Combustible corrosive hazardous materials

wgk

WGK 3

ppe

Eyeshields, Faceshields, Gloves, type P3 (EN 143) respirator cartridges

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Certificates of Analysis (COA)

Lot/Batch Number
MKCV0043
MKCH6467
MKCG2415
MKCF4214
MKCB1936V

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A convenient 'catch and release' synthesis of fused 2-alkylthio-pyrimidinones mediated by polymer-bound BEMP.
Gregory L. Adams et al.
Tetrahedron Letters, 44, 5041-5045 (2003)
A study of polymer-supported bases for the solution phase synthesis of glycosyl trichloroacetimidates.
Jose Luis Chiara, Lourdes Encinas and Beatriz Diaz
Tetrahedron Letters, 46, 2445-2448 (2005)
Serena Gabrielli et al.
Molecules (Basel, Switzerland), 21(6) (2016-06-18)
Quinoline-2-carboxylates are an important subclass of quinoline derivatives largely present in a variety of biologically active molecules, as well as useful ligands in metal-catalyzed reactions. Herein, we present a new one-pot protocol for synthesizing this class of derivatives starting from
Ying Wang et al.
Organic letters, 7(5), 925-928 (2005-02-25)
1,2,4-Oxadiazoles can be rapidly and efficiently synthesized from a variety of readily available carboxylic acids and amidoximes using either method A or method B. The use of commercially available polymer-supported reagents combined with microwave heating resulted in high yields and

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