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2-Butanone ethylene ketal, 2-Ethyl-2-methyl-1,3-dioxolane, 2-Ethyl-2-methyldioxolane, 2-Methyl-2-ethyl-1,3-dioxolane, 2-Methyl-2-ethyldioxolane
C6H12O2
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Quality Level
Assay
99%
form
liquid
refractive index
n20/D 1.409 (lit.)
bp
116-117 °C (lit.)
density
0.929 g/mL at 25 °C (lit.)
SMILES string
CCC1(C)OCCO1
InChI
1S/C6H12O2/c1-3-6(2)7-4-5-8-6/h3-5H2,1-2H3
InChI key
UPZFLZYXYGBAPL-UHFFFAOYSA-N
Related Categories
Application
2-Ethyl-2-methyl-1,3-dioxolane was employed as reagent in the selective ketalization of 1-oxo functions of 8a-methyl 1,6-dioxo 1,2,3,4,6,7,8,8a-octahydronaphthalene and 7a-methyl 1,5-dioxo 5,6,7,7a-tetrahydroindane. It was also employed in the enantioselective total synthesis of (-)-strychnine.
Signal Word
Danger
Hazard Statements
Precautionary Statements
Hazard Classifications
Acute Tox. 4 Inhalation - Eye Irrit. 2 - Flam. Liq. 2 - Skin Irrit. 2 - STOT SE 3
Target Organs
Respiratory system
WGK
WGK 3
Flash Point(F)
55.4 °F
Flash Point(C)
13 °C
Personal Protective Equipment
dust mask type N95 (US), Eyeshields, Gloves
Regulatory Information
危险化学品
Certificates of Analysis (COA)
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Etudes en series bicycliques: Cetalisation selective de dicetones octalinique et tetrahydroindanique et stereochimie de leurs analogues satures.
Tetrahedron, 29(24), 4225-4231 (1973)
Journal of the American Chemical Society, 124(49), 14546-14547 (2002-12-06)
The enantioselective total synthesis of (-)-strychnine was accomplished through the use of the highly practical catalytic asymmetric Michael reaction (0.1 mol % of (R)-ALB, more than kilogram scale, without chromatography, 91% yield and >99% ee) as well as a tandem
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