305227
Phenyl vinylsulfonate
95%
Synonym(s):
Phenyl ethylenesulfonate, Vinylsulfonic acid phenyl ester
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About This Item
Linear Formula:
CH2=CHSO3C6H5
CAS Number:
Molecular Weight:
184.21
Beilstein:
2044718
MDL number:
UNSPSC Code:
12352100
PubChem Substance ID:
NACRES:
NA.22
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Assay
95%
bp
44-46 °C/2 mmHg (lit.)
mp
38-42 °C (lit.)
SMILES string
C=CS(=O)(=O)Oc1ccccc1
InChI
1S/C8H8O3S/c1-2-12(9,10)11-8-6-4-3-5-7-8/h2-7H,1H2
InChI key
CILDJVVXNMDAGY-UHFFFAOYSA-N
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General description
Phenyl vinylsulfonate is an ester. Palladium complex derived from a tetraphosphine-catalyzed Heck vinylation of phenyl vinylsulfonate was reported. Phenyl vinyl sulfonate reacts with various alkyl furan derivatives to yield the corresponding cycloadducts.
Signal Word
Warning
Hazard Statements
Precautionary Statements
Hazard Classifications
Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
Target Organs
Respiratory system
Storage Class Code
11 - Combustible Solids
WGK
WGK 3
Flash Point(F)
230.0 °F - closed cup
Flash Point(C)
110 °C - closed cup
Personal Protective Equipment
dust mask type N95 (US), Eyeshields, Gloves
Regulatory Information
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Heck vinylations using vinyl sulfide, vinyl sulfoxide, vinyl sulfone, or vinyl sulfonate derivatives and aryl bromides catalyzed by a palladium complex derived from a tetraphosphine.
Battace A, et al.
Synthesis, 2006(20), 3495-3505 (2006)
Mild and practical cycloaddition reactions of furans with phenyl vinyl sulfonate.
Klein LL and Deeb TM.
Tetrahedron Letters, 26(33), 3935-3938 (1985)
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