211478
1-Bromo-2,4-dimethylbenzene
97%
Synonym(s):
4-Bromo-m-xylene
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About This Item
Linear Formula:
(CH3)2C6H3Br
CAS Number:
Molecular Weight:
185.06
EC Number:
MDL number:
UNSPSC Code:
12352100
PubChem Substance ID:
NACRES:
NA.22
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Assay
97%
form
liquid
refractive index
n20/D 1.551 (lit.)
bp
214 °C (lit.)
density
1.37 g/mL at 25 °C (lit.)
functional group
bromo
SMILES string
Cc1ccc(Br)c(C)c1
InChI
1S/C8H9Br/c1-6-3-4-8(9)7(2)5-6/h3-5H,1-2H3
InChI key
YSFLQVNTBBUKEA-UHFFFAOYSA-N
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General description
Gold-catalyzed coupling reaction of pyrazine with 1-bromo-2,4-dimethylbenzene has been reported. 1-Bromo-2,4-dimethylbenzene reacts with Mg and DMF, followed by the reaction with I2 and aq.NH3 to afford the corresponding aromatic nitrile.
Signal Word
Warning
Hazard Statements
Precautionary Statements
Hazard Classifications
Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
Target Organs
Respiratory system
Storage Class Code
10 - Combustible liquids
WGK
WGK 3
Flash Point(F)
174.2 °F - closed cup
Flash Point(C)
79 °C - closed cup
Personal Protective Equipment
dust mask type N95 (US), Eyeshields, Gloves
Regulatory Information
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Gold (I)-catalyzed direct C-H arylation of pyrazine and pyridine with aryl bromides.
Li M and Hua R.
Tetrahedron Letters, 50(13), 1478-1481 (2009)
Transformation of aromatic bromides into aromatic nitriles via formations of grignard reagents and their DMF adducts.
Ishii G, et al.
Tetrahedron Letters, 52(18), 2404-2406 (2011)
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