试验参数
column: Astec Cellulose DMP, 25 cm x 4.6 mm I.D., 5 μm particles (51099AST)
mobile phase: [A] CO2; [B] methanol containing 0.1% DEA in CO2; (75:25, A:B)
flow rate: 3 mL/min
pressure: 1740 psi (120 bar)
detector: UV, 230 nm
injection: 5 μL
sample: 2 mg/mL in methanol
适用性
application for SFC
应用
pharmaceutical (small molecule)
分析说明
This application demonstrates the ability of the Astec® Cellulose DMP column to separate Aminoglutethimide enantiomers via Supercritical Fluid Chromatography. DMPC-derivatized cellulose is widely used for chiral separations by SFC, both analytical and prep. The Astec® Cellulose DMP works well in SFC mode, providing rapid separations with excellent selectivity.
法律信息
Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
分析物
说明
DL-Aminoglutethimide
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