236330
对甲苯磺酰胺
ReagentPlus®, ≥99%
别名:
4-Methylbenzene-1-sulfonamide, p-Tosylamide
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关于此项目
线性分子式:
CH3C6H4SO2NH2
化学文摘社编号:
分子量:
171.22
UNSPSC Code:
12352100
NACRES:
NA.22
PubChem Substance ID:
EC Number:
200-741-1
Beilstein/REAXYS Number:
472689
MDL number:
Assay:
≥99%
Form:
solid
产品名称
对甲苯磺酰胺, ReagentPlus®, ≥99%
InChI key
LMYRWZFENFIFIT-UHFFFAOYSA-N
InChI
1S/C7H9NO2S/c1-6-2-4-7(5-3-6)11(8,9)10/h2-5H,1H3,(H2,8,9,10)
SMILES string
Cc1ccc(cc1)S(N)(=O)=O
product line
ReagentPlus®
assay
≥99%
form
solid
mp
134-137 °C (lit.)
Quality Level
Gene Information
human ... CA1(759), CA2(760), CA5A(763), CA5B(11238)
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Application
p -甲苯磺酰胺已被用作：
- 四丁基氟化铵 (TBAF) 催化乙烯基氮丙啶开环反应中的亲核试剂
- 己内酰胺二铑 (II) 催化烯烃氮杂环丙烷化反应的试剂
General description
研究了氰甲基三丁基磷 (CMBP) 介导的 对 甲苯磺酰胺与醇的反应 。
Legal Information
ReagentPlus is a registered trademark of Merck KGaA, Darmstadt, Germany
存储类别
11 - Combustible Solids
wgk
WGK 1
flash_point_f
395.6 °F - closed cup
flash_point_c
202 °C - closed cup
ppe
dust mask type N95 (US), Eyeshields, Gloves
Arthur J Catino et al.
Organic letters, 7(13), 2787-2790 (2005-06-17)
[reaction: see text] A mild, efficient, and selective aziridination of olefins catalyzed by dirhodium(II) caprolactamate [Rh(2)(cap)(4).2CH(3)CN] is described. Use of p-toluenesulfonamide (TsNH(2)), N-bromosuccinimide (NBS), and potassium carbonate readily affords aziridines in isolated yields of up to 95% under extremely mild
E Simone et al.
Lab on a chip, 18(15), 2235-2245 (2018-06-28)
In this work, a novel multi-microfluidic crystallization platform called MMicroCryGen is presented, offering a facile methodology for generating individual crystals for fast and easy screening of the polymorphism and crystal habit of solid compounds. The MMicroCryGen device is capable of
Mitsunobu-type alkylation of p-toluenesulfonamide. A convenient new route to primary and secondary amines.
Tsunoda T, et al.
Tetrahedron Letters, 37(!4), 2457-2458 (1996)
An efficient FeCl3 -catalyzed amidation reaction of secondary benzylic and allylic alcohols with carboxamides or p-toluenesulfonamide.
Jana U, et al.
Tetrahedron Letters, 42(37), 6433-6435 (2001)
Yang Yang et al.
Organic letters, 13(20), 5608-5611 (2011-09-16)
BF(3)·OEt(2)-catalyzed direct cyanation of indoles and pyrroles using a less toxic, bench-stable, and easily handled electrophilic cyanating agent N-cyano-N-phenyl-para-toluenesulfonamide (NCTS) affords 3-cyanoindoles and 2-cyanopyrroles in good yields with excellent regioselectivity. The substrate scope is broad with respect to indoles and
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