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GC Analysis of Solvents in Water on SPB®-1 SULFUR after SPME using 75 μm Carboxen/PDMS Fiber

GC Analysis of Solvents in Water on SPB®-1 SULFUR after SPME using 75 μm Carboxen/PDMS Fiber suitable for GC, application for SPME

Materials

analytical column

Product No.
Description
Pricing

24158

SPB®-1 SULFUR Capillary GC Column

L × I.D. 30 m × 0.32 mm, df 4.00 μm

SPME fiber

Product No.
Description
Pricing

57318

SPME fiber assembly Carboxen/Polydimethylsiloxane (CAR/PDMS)

df 75 μm(CAR/PDMS, for use with manual holder, needle size 24 ga

CONDITIONS

sample/matrix

solvents at 20 ppb in 4 mL water + 25% NaCl in 4 mL vial

SPME fiber

carboxen/PDMS, 75 μm (57318)

extraction

immersion, 10 min, rapid stirring

desorption process

270 °C, 5 min

column

SPB-1 SULFUR, 30 m × 0.32 mm I.D., 4.0 μm film (24158)

oven

50°C (2 min) to 150°C at 10°C/min

inj. temp.

splitless (closed 2 min), 260°C, 0.75 mm I.D. liner

detector

FID

carrier gas

helium, 30 cm/sec

Description

Legal Information

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

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Related Product Categories

HPLC ColumnsGC Columns & AccessoriesTLC Plates & AdsorbentsSolid Phase Microextraction (SPME)Solid Phase Extraction & QuEChERS

Related Applications

Small Molecule HPLCLarge Molecule HPLCGas Chromatography (GC)TLCSolid Phase Microextraction (SPME)Solid Phase Extraction (SPE)QuEChERS