GC Analysis of (R)-(+)-1-Phenylethylamine (N-Trifluoroacetyl Derivative) on Astec® CHIRALDEX™ G-PN
Materials
analytical column
Product No.
Description
Pricing
CONDITIONS
column
Astec CHIRALDEX G-PN, 30 m x 0.25 mm I.D., 0.12 μm (74033AST)
oven
130 °C
inj. temp.
250 °C
detector
FID, 250 °C
carrier gas
helium, 30 psi
injection
1 μL, 80:1 split
sample
3 mg/mL in methanol
peak 1: (R)-(+)-1-phenylethylamine (N-TFA derivative) (ee% 99.1)
peak 2: (S)-(-)-1-phenylethylamine (N-TFA derivative)
Description
Legal Information
Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC