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GC Analysis of Amphetamine Enantiomers (N-Trifluoroacetyl Derivative) on Astec® CHIRALDEX™ G-PN

GC Analysis of Amphetamine Enantiomers (N-Trifluoroacetyl Derivative) on Astec® CHIRALDEX™ G-PN suitable for GC

Materials

analytical column

Product No.
Description
Pricing

74033AST

Astec® CHIRALDEX™ G-PN Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.12 μm

Application

Product No.
Description
Pricing

G005151

GC Analysis of Amphetamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX™ G-DP

suitable for GC

standard

Product No.
Description
Pricing

A3278

D-Amphetamine hemisulfate salt solution

1.0 mg/mL in methanol, analytical standard, for drug analysis

A1263

DL-Amphetamine sulfate salt

A5880

D-Amphetamine hemisulfate salt

94777

DL-Amphetamine hydrochloride

analytical standard

CONDITIONS

column

Astec CHIRALDEX G-PN, 30 m x 0.25 mm I.D., 0.12 μm (74033AST)

oven

130 °C

detector

FID, 250 °C

carrier gas

helium, 30 psi

inj. temp.

250 °C

liner

4 mm I.D., double taper

sample

peak 1: l-amphetamine (N-TFA)
peak 2: d-amphetamine (N-TFA)

Description

Analysis Note

Achieve elution order reversal (d,l) by using CHIRALDEX G-DP column, 140 °C (see G005151).

Legal Information

Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC

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