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  • Development and validation of an ultra performance liquid chromatography Q-Exactive Orbitrap mass spectrometry for the determination of fipronil and its metabolites in tea and chrysanthemum.

Development and validation of an ultra performance liquid chromatography Q-Exactive Orbitrap mass spectrometry for the determination of fipronil and its metabolites in tea and chrysanthemum.

Food chemistry (2018-01-03)
Hongping Chen, Guanwei Gao, Pingxiang Liu, Meiling Pan, Yunfeng Chai, Xin Liu, Chengyin Lu
ABSTRACT

A fast, sensitive and reliable method for the determination of fipronil and its metabolites in tea and chrysanthemum was developed using a modified QuEChERS technique and an ultra performance liquid chromatography Q-Exactive Orbitrap mass spectrometry. The mixture of adsorbents containing primary secondary amine (PSA), octadecylsilane (C

MATERIALS
Product Number
Brand
Product Description

Supelco
Fipronil-desulfinyl, PESTANAL®, analytical standard