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GLC-mass spectral analysis of psilocin and psilocybin.

Journal of pharmaceutical sciences (1977-05-01)
D B Repke, D T Leslie, D M Mandell, N G Kish
PMID559753
ABSTRACT

With the combined technique of GLC-mass spectrometry, psilocin and psilocybin, two hallucinogenic indoles, were analyzed as their trimethylsilyl derivatives. The method was applied to these two components in an extract of Psilocybe cubensis (Earle) Sing.