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Merck
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UHPLC-MS溶剂和LC-MS试剂,时刻追求更高的灵敏度

确保可靠结果,质谱分析新标杆-Advanced LC-MS Solvents & Reagents

Highest Purity Solvents for UHPLC-MS Analysis

在进行高度灵敏的UHPLC-MS分析时,如何才能最大限度地降低噪音及其他信号?我们全新的高端UHPLC-MS溶剂以其低基线噪音和高质谱清晰度而树立了新标杆。该溶剂先进技术生产,性能超出所有预期,不论在ESI/APCI +还是-电离模式下都能确保快速可靠地获得结果。

由于其背景噪音及离子抑制水平极低,电离效率好,灵敏度高,同时也延长了色谱柱的使用寿命。所有UHPLC-MS溶剂都最大程度地降低了聚乙二醇(PEG)杂质的含量限值,确保您对结果充满信心。该产品可满足科研及质检领域中高规格的UHPLC-MS要求,例如蛋白质组学、代谢组学以及环境、临床、食品或工业检测等应用。

特点和优势

  • 专为UHPLC-MS和UHPLC-UV而设计,并进行了相应的适用性测试,确保分析灵活性
  • 在+/-ESI及APCI MS模式下性能稳定,在任何重要的MS模式下均可确保低检测限和分析置信度(测试1)
    ––ESI/APCI (+) < 2 ppb
    ––ESI/APCI (-) < 10 ppb
  • 杂质含量极低:确保无干扰的基线(测试2)
  • 采用0.2 μm滤器过滤(测试3)
    ––延长HPLC系统中滤器及机械组件的寿命
    ––降低色谱柱的堵塞风险
  • 采用硼硅酸盐玻璃瓶包装:最大限度降低金属离子污染
  • 设计为GL45瓶口,可方便直接与仪器连接
  • 痕量金属杂质含量低:最大限度减少金属离子加合物的形成
    ––<5ppb
  • 我们所有UHPLC-MS溶剂产品的聚乙二醇(PEG)杂质含量都极低,能确保可靠的分析结果(PEG的S/N信噪比<50)

订购信息

Cat. No.
货号
Description
产品
1037251002Acetonitrile for UHPLC-MS
1037252002Acetonitrile for UHPLC-MS
1037261002Methanol for UHPLC-MS
1037262002Methanol for UHPLC-MS
1037281002Water for UHPLC-MS
1037282002Water for UHPLC-MS
00922-10x1mLDifluoroacetic acid for LC-MS
00922-1mLDifluoroacetic acid for LC-MS
00922-50mLDifluoroacetic acid for LC-MS
18127-10mLHexafluoroisopropanol for LC-MS
18127-50mLHexafluoroisopropanol for LC-MS
5330010050Acetic acid for LC-MS
5330030050Ammonia solutions for LC-MS
70221-100G-FAmmoniumformate for LC-MS
70221-25G-FAmmoniumformate for LC-MS
80457-10mLTrifluoracetic acid for LC-MS
80457-10x1mLTrifluoracetic acid for LC-MS
80457-50mLTrifluoracetic acid for LC-MS
900666-100mLBruker standard solvent, for MALDI MS, 50%ACN, 47,5% H2O + 2,5% TFA
900666-250mLBruker standard solvent, for MALDI MS, 50%ACN, 47,5% H2O + 2,5% TFA
900667-100mLAcetonitrile for UHPLC, for mass spectrometry
900667-1LAcetonitrile for UHPLC, for mass spectrometry
900667-250mLAcetonitrile for UHPLC, for mass spectrometry
900667-4x4LAcetonitrile for UHPLC, for mass spectrometry
900682-1LWater for UHPLC, for mass spectrometry
900682-4x4LWater for UHPLC, for mass spectrometry
900682-6x1LWater for UHPLC, for mass spectrometry
900686-1LAcetonitril solution contains 0.1% formic acid
900686-4x4LAcetonitril solution contains 0.1% formic acid
900687-1LWater solution contains 0.1% formic acid
900687-4x4LWater solution contains 0.1% formic acid
900688-1LMethanol for UHPLC, for mass spectrometry
900688-4x4LMethanol for UHPLC, for mass spectrometry
900688-6x1LMethanol for UHPLC, for mass spectrometry
Figure 1. UHPLC-MS chromatograms showing that the signals for 500 ppt propazine, 1 ppb reserpine, and 4 ppb prednisolone are all higher than the background signal.

Figure 1. UHPLC-MS chromatograms showing that the signals for 500 ppt propazine, 1 ppb reserpine, and 4 ppb prednisolone are all higher than the background signal.

测试一

Detection limit analysis for UHPLC-MS solvents

采用UHPLC-MS的LiChrosolv®乙腈进行的UHPLC-MS梯度测试表明,可在极低的背景干扰下清晰检测和鉴定1 ppb利血平(Reserpine)、500 ppt扑灭津(Propazine)以及4 ppb泼尼松龙(Pprednisolone)。

测试条件:

采用UHPLC-MS的LiChrosolv®乙腈和LiChrosolv®水进行从2%乙腈至98%乙腈的UHPLC-MS梯度洗脱。UHPLC色谱柱:Supelco Ascentis® Express C18,2 μm,2.1 x 30 mm。MS仪器类型:Q-TOF。检测模式:ESI (+)。


Figure 2. UHPLC-MS chromatograms comparing the baseline of our high purity ® solvents against those of two competitors.

Figure 2. UHPLC-MS chromatograms comparing the baseline of our high purity ® solvents against those of two competitors.

测试二

Methanol UHPLC-MS solvent baseline competitor comparison

将UHPLC-MS的LiChrosolv®甲醇(蓝线)与其他两种UHPLC-MS品牌进行比较。

UHPLC-MS的LiChrosolv®甲醇表现出了平稳的基线以及与其他品牌相比最低的杂质含量(截至目前)。两款高纯度UHPLC-MS品牌A和B都表现出了基线漂移及显著的杂质峰。

测试条件:

采用UHPLC-MS的LiChrosolv®甲醇和LiChrosolv®水进行从2%甲醇至98%甲醇的UHPLC-MS梯度洗脱。UHPLC色谱柱:Supelco Ascentis® Express C18,2 μm,2.1 x 30 mm。检测模式:ToF-MS(ESI (+))。


Figure 3. Particle size analysis in LiChrosolv® acetonitrile for UHPLC-MS versus an equivalent competitor UHPLC-MS grade solvent.

Figure 3. Particle size analysis in LiChrosolv® acetonitrile for UHPLC-MS versus an equivalent competitor UHPLC-MS grade solvent.

测试三

Acetonitrile UHPLC-MS solvent particle size competitor comparison

对UHPLC-MS的LiChrosolv®乙腈及另一款UHPLC-MS级溶剂品牌进行颗粒浓度测量。颗粒浓度按不同的粒径范围进行划分。在所有分析的粒径范围中,品牌C均展现出了明显更高的颗粒浓度。低颗粒浓度可延长HPLC系统中滤器及机械组件的寿命,并降低色谱柱堵塞的危险。而高颗粒浓度则相反,并可能会造成对杂质的检测。

测试条件:

溶剂样品采用基于光衍射技术的颗粒计数器(RION KS-40BF)进行五次测量。

SolventSupplier> 0.2 µm Particles/10 mL> 0.3 µm Particles/10 mL0.5 µm Particles/10 mL1 µm Particles/10 mL2 µm Particles/10 mL
AcetonitrileMerck 2 784 ± 58828 ± 1583 ± 79 ± 3.20.6 ± 0.49
 Competitor C> 12 000> 12 000> 12 0002 054 ± 52456 ± 19
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