1.04874
Potassium hydrogen phthalate
for analysis EMSURE® Reag. Ph Eur
Recommended Products
Agency
reag. Ph. Eur.
Quality Level
product line
EMSURE®
Assay
≥99.5% dry basis (perchloric acid titration)
form
solid
potency
>3200 mg/kg LD50, oral (Rat)
impurities
≤0.005% In water insoluble matter
loss
≤0.2% loss on drying, 105°C
pH
4.0 (20 °C, 50 g/L in H2O)
mp
295-300 °C
density
1.636 g/cm3
bulk density
900 kg/m3
anion traces
chloride (Cl-): ≤0.002%
sulfur compounds (as SO42-): ≤0.005%
cation traces
Cu: ≤0.0002%
Fe: ≤0.0005%
Na: ≤0.01%
Pb: ≤0.0005%
heavy metals (as Pb): ≤0.0005%
storage temp.
2-30°C
InChI
1S/C8H6O4.K/c9-7(10)5-3-1-2-4-6(5)8(11)12;/h1-4H,(H,9,10)(H,11,12);/q;+1/p-1
InChI key
IWZKICVEHNUQTL-UHFFFAOYSA-M
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Application
- Coulometric method with titratable impurity analysis and mass balance method: This study presents a method to convert acidimetric purity to chemical purity for potassium hydrogen phthalate, which is validated using quantitative nuclear magnetic resonance (qNMR) techniques, enhancing the standards for analytical chemistry (Huang T et al., 2023).
- Triplet states of the nonlinear optical chromophore DCM in single crystals: Investigates the triplet excited states of the nonlinear optical chromophore DCM in potassium hydrogen phthalate single crystals, linking these states to single-molecule dark states, significant for the development of optical materials (Barbon A et al., 2009).
Analysis Note
Identity (IR-spectrum): passes test
In water insoluble matter: ≤ 0.005 %
Chloride (Cl): ≤ 0.002 %
Sulfur compounds (as SO₄): ≤ 0.005 %
Heavy metals (as Pb): ≤ 0.0005 %
Cu (Copper): ≤ 0.0002 %
Fe (Iron): ≤ 0.0005 %
Na (Sodium): ≤ 0.01 %
Pb (Lead): ≤ 0.0005 %
Loss on Drying (105°C): ≤ 0.2 %
Corresponds to Reag. Ph Eur
Legal Information
Storage Class Code
11 - Combustible Solids
WGK
WGK 1
Flash Point(F)
387.1 °F - Pensky-Martens closed cup
Flash Point(C)
197.3 °C - Pensky-Martens closed cup
Certificates of Analysis (COA)
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Protocols
Photometric determination using the Griess method subsequent to extraction
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